Information card for entry 2232698

Structure parameters

• Chemical name: <i>catena</i>-Poly[[lead(II)-μ-<i>N</i>'-[1-(pyridin-2- yl-κ<i>N</i>)ethylidene]isonicotinohydrazidato- κ^3^<i>N</i>',<i>O</i>:<i>N</i>^1^] perchlorate]
• Formula: C13 H11 Cl N4 O5 Pb
• Calculated formula: C13 H11 Cl N4 O5 Pb
• SMILES: [Pb]12(OC(=N[N]2=C(c2[n]1cccc2)C)c1ccncc1)[n]1ccc(C2O[Pb]3[n]4c(cccc4)C(=[N]3N=2)C)cc1.Cl(=O)(=O)(=O)[O-].Cl(=O)(=O)(=O)[O-]
• Title of publication: <i>catena</i>-Poly[[lead(II)-μ-<i>N</i>'-[1-(pyridin-2-yl-κ<i>N</i>)ethylidene]isonicotinohydrazidato-κ^3^<i>N</i>',<i>O</i>:<i>N</i>^1^] perchlorate]
• Authors of publication: Shahverdizadeh, Gholam Hossein; Tiekink, Edward R. T.; Mirtamizdoust, Babak
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1727 - m1728
• a: 10.062 ± 0.0006 Å
• b: 14.4431 ± 0.0008 Å
• c: 11.1456 ± 0.0007 Å
• α: 90°
• β: 99.174 ± 0.001°
• γ: 90°
• Cell volume: 1599.03 ± 0.16 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0315
• Residual factor for significantly intense reflections: 0.0222
• Weighted residual factors for significantly intense reflections: 0.0509
• Weighted residual factors for all reflections included in the refinement: 0.0555
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes