Information card for entry 2232706

Structure parameters

• Chemical name: Bis{1,2-bis[bis(3-methoxypropyl)phosphanyl]ethane-\ κ^2^<i>P</i>,<i>P</i>'}dichloridoosmium(II)
• Formula: C36 H80 Cl2 O8 Os P4
• Calculated formula: C36 H80 Cl2 O8 Os P4
• Title of publication: Bis{1,2-bis[bis(3-methoxypropyl)phosphanyl]ethane-κ^2^<i>P</i>,<i>P</i>'}dichloridoosmium(II)
• Authors of publication: Szymczak, Nathaniel K.; Zakharov, Lev N.; Tyler, David R.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1808
• a: 12.667 ± 0.003 Å
• b: 10.321 ± 0.002 Å
• c: 18.754 ± 0.004 Å
• α: 90°
• β: 107.779 ± 0.003°
• γ: 90°
• Cell volume: 2334.7 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0339
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0531
• Weighted residual factors for all reflections included in the refinement: 0.0579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes