Information card for entry 2232871

Structure parameters

• Chemical name: Tris(tetrahydrofuran-κ<i>O</i>)tris[tris(thiophen-2-yl)methanolato- κ<i>O</i>]terbium(III) tetrahydrofuran monosolvate
• Formula: C55 H59 O7 S9 Tb
• Calculated formula: C54.99 H58.92 O7 S9 Tb
• Title of publication: Tris(tetrahydrofuran-κ<i>O</i>)tris[tris(thiophen-2-yl)methanolato-κ<i>O</i>]terbium(III) tetrahydrofuran monosolvate
• Authors of publication: Veith, Michael; Belot, Celine; Huch, Volker
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1712
• a: 13.9131 ± 0.0004 Å
• b: 13.9131 ± 0.0004 Å
• c: 24.6789 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4137.2 ± 0.2 ų
• Cell temperature: 132 ± 2 K
• Ambient diffraction temperature: 132 ± 2 K
• Number of distinct elements: 5
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.085
• Weighted residual factors for all reflections included in the refinement: 0.0852
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes