Information card for entry 2232970

Structure parameters

• Chemical name: Tris(4,4'-di-<i>tert</i>-butyl-2,2'-bipyridine- κ^2^<i>N</i>,<i>N</i>')molybdenum(II) μ~6~-oxido-dodeca-μ~2~-oxido-hexaoxidohexamolybdate(VI) acetonitrile tetrasolvate
• Formula: C62 H84 Mo7 N10 O19
• Calculated formula: C62 H84 Mo7 N10 O19
• Title of publication: Tris(4,4'-di-<i>tert</i>-butyl-2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')molybdenum(II) μ~6~-oxido-dodeca-μ~2~-oxido-hexaoxidohexamolybdate(VI) acetonitrile tetrasolvate
• Authors of publication: Amarante, Tatiana R.; Fernandes, José A.; Gonçalves, Isabel S.; Almeida Paz, Filipe A.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1828 - m1829
• a: 14.4202 ± 0.0008 Å
• b: 16.3205 ± 0.0009 Å
• c: 17.1122 ± 0.001 Å
• α: 90.144 ± 0.003°
• β: 103.862 ± 0.002°
• γ: 107.547 ± 0.002°
• Cell volume: 3715.9 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1347
• Weighted residual factors for all reflections included in the refinement: 0.1486
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes