Information card for entry 2232994

Structure parameters

• Chemical name: Tetrakis(3-cyanopyridine-κ<i>N</i>^1^)bis(thiocyanato-κ<i>N</i>)cobalt(II) 1,4-dioxane disolvate
• Formula: C34 H32 Co N10 O4 S2
• Calculated formula: C34 H32 Co N10 O4 S2
• Title of publication: Tetrakis(3-cyanopyridine-κ<i>N</i>^1^)bis(thiocyanato-κ<i>N</i>)cobalt(II) 1,4-dioxane disolvate
• Authors of publication: Diehr, Stephan; Wöhlert, Susanne; Boeckmann, Jan; Näther, Christian
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1898
• a: 15.5222 ± 0.0006 Å
• b: 14.1865 ± 0.0007 Å
• c: 10.0762 ± 0.0004 Å
• α: 90°
• β: 124.454 ± 0.003°
• γ: 90°
• Cell volume: 1829.61 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.0943
• Weighted residual factors for all reflections included in the refinement: 0.0979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.166
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes