Information card for entry 2233047

Structure parameters

• Chemical name: <i>cis</i>-Bis(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')bis(dimethyl sulfoxide-κ<i>O</i>)zinc bis(tetraphenylborate) dimethyl sulfoxide monosolvate
• Formula: C74 H74 B2 N4 O3 S3 Zn
• Calculated formula: C74 H74 B2 N4 O3 S3 Zn
• Title of publication: <i>cis</i>-Bis(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')bis(dimethyl sulfoxide-κ<i>O</i>)zinc bis(tetraphenylborate) dimethyl sulfoxide monosolvate
• Authors of publication: Tomyn, Stefania; Gumienna-Kontecka, Elżbieta; Usenko, Natalia I.; Iskenderov, Turganbay S.; Prisyazhnaya, Elena V.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1774 - m1775
• a: 13.8836 ± 0.0005 Å
• b: 18.0029 ± 0.0007 Å
• c: 26.1594 ± 0.001 Å
• α: 90°
• β: 90.225 ± 0.003°
• γ: 90°
• Cell volume: 6538.4 ± 0.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0812
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.0947
• Goodness-of-fit parameter for all reflections included in the refinement: 0.941
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes