Information card for entry 2233977

Structure parameters

• Common name: bis(triphenylsilyl) oxide toluene disolvate
• Chemical name: triphenyl[(triphenylsilyl)oxy]silane toluene disolvate
• Formula: C50 H46 O Si2
• Calculated formula: C50 H46 O Si2
• SMILES: c1(ccccc1)[Si](c1ccccc1)(O[Si](c1ccccc1)(c1ccccc1)c1ccccc1)c1ccccc1.c1ccc(cc1)C.c1ccc(cc1)C
• Title of publication: Triclinic polymorph of bis(triphenylsilyl) oxide toluene disolvate
• Authors of publication: Purdy, Andrew P.; Smoot, Emily; Butcher, Ray J.; Kerr, Andrew
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 3
• Pages of publication: o588
• a: 10.756 ± 0.003 Å
• b: 11.062 ± 0.003 Å
• c: 11.156 ± 0.003 Å
• α: 62.638 ± 0.004°
• β: 61.356 ± 0.004°
• γ: 61.795 ± 0.004°
• Cell volume: 978.9 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1187
• Residual factor for significantly intense reflections: 0.0884
• Weighted residual factors for significantly intense reflections: 0.2367
• Weighted residual factors for all reflections included in the refinement: 0.259
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes