Information card for entry 2234259

Structure parameters

• Chemical name: Bis[μ-<i>N</i>-(3-methoxy-2-oxidobenzylidene-1:2κ^2^<i>O</i>^2^:<i>O</i>^2^)- L-isoleucinato-2κ^2^<i>N</i>,<i>O</i>]bis(1,10-phenanthroline- 1κ^2^<i>N</i>,<i>N</i>')dinickel(II) methanol tetrasolvate trihydrate
• Formula: C56 H72 N6 Ni2 O15
• Calculated formula: C56 H72 N6 Ni2 O15
• Title of publication: Bis[μ-<i>N</i>-(3-methoxy-2-oxidobenzylidene-1:2κ^2^<i>O</i>^2^:<i>O</i>^2^)-<small>L</small>-isoleucinato-2κ^2^<i>N</i>,<i>O</i>]bis(1,10-phenanthroline-1κ^2^<i>N</i>,<i>N</i>')dinickel(II) methanol tetrasolvate trihydrate
• Authors of publication: Li, Yan; Guo, Zhenghua; Dong, Jianfang; Li, Lianzhi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 4
• Pages of publication: m371 - m372
• a: 14.1827 ± 0.0015 Å
• b: 14.3876 ± 0.0016 Å
• c: 28.787 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5874.1 ± 1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0865
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1358
• Weighted residual factors for all reflections included in the refinement: 0.1573
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes