Information card for entry 2234480

Structure parameters

• Chemical name: 2,4-Bis(diphenylphosphanyl)-1,1,2,3,3,4-hexaphenyl- 1,3-diphospha-2,4-diboracyclobutane tetrahydrofuran sesquisolvate
• Formula: C66 H62 B2 O1.5 P4
• Calculated formula: C66 H62 B2 O1.5 P4
• Title of publication: 2,4-Bis(diphenylphosphanyl)-1,1,2,3,3,4-hexaphenyl-1,3-diphospha-2,4-diboracyclobutane tetrahydrofuran sesquisolvate
• Authors of publication: Peulecke, Normen; Müller, Bernd H.; Spannenberg, Anke; Rosenthal, Uwe
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 4
• Pages of publication: o1125
• a: 19.2421 ± 0.0004 Å
• b: 11.6938 ± 0.0002 Å
• c: 24.9769 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5620.13 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0732
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0895
• Weighted residual factors for all reflections included in the refinement: 0.0958
• Goodness-of-fit parameter for all reflections included in the refinement: 0.867
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes