Information card for entry 2234867

Structure parameters

• Chemical name: Bis[2-(2-oxoindolin-3-ylidene)-<i>N</i>-phenylhydrazinecarbothioamidato- κ^3^<i>O</i>,<i>N</i>^2^,<i>S</i>]nickel(II) dimethylformamide monosolvate
• Formula: C33 H29 N9 Ni O3 S2
• Calculated formula: C33 H29 N9 Ni O3 S2
• Title of publication: Bis[2-(2-oxoindolin-3-ylidene)-<i>N</i>-phenylhydrazinecarbothioamidato-κ^3^<i>O</i>,<i>N</i>^2^,<i>S</i>]nickel(II) dimethylformamide monosolvate
• Authors of publication: Ali, Amna Qasem; Eltayeb, Naser Eltaher; Teoh, Siang Guan; Salhin, Abdussalam; Fun, Hoong-Kun
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 5
• Pages of publication: m538 - m539
• a: 12.2491 ± 0.0002 Å
• b: 12.317 ± 0.0003 Å
• c: 13.1142 ± 0.0002 Å
• α: 104.854 ± 0.001°
• β: 112.943 ± 0.001°
• γ: 102.798 ± 0.001°
• Cell volume: 1642.31 ± 0.06 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0583
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0972
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes