Information card for entry 2235146

Structure parameters

• Chemical name: bis(μ-<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato)- κ^3^<i>O</i>,<i>O</i>':<i>O</i>';κ^3^<i>O</i>':<i>O</i>,<i>O</i>'- bis[(<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato- κ^2^<i>O</i>,<i>O</i>')lead(II)]
• Formula: C24 H20 N8 O8 Pb2
• Calculated formula: C24 H20 N8 O8 Pb2
• SMILES: [Pb]123([O]=NN(c4ccccc4)O1)[O]=NN(c1ccccc1)[O]2[Pb]12([O]=NN(c4ccccc4)O1)[O]=NN(c1ccccc1)[O]23
• Title of publication: A second triclinic polymorph of bis(μ-<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato)-κ^3^<i>O</i>,<i>O</i>':<i>O</i>';κ^3^<i>O</i>':<i>O</i>,<i>O</i>'-bis[(<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato-κ^2^<i>O</i>,<i>O</i>')lead(II)]
• Authors of publication: Najafi, Ezzatollah; Amini, Mostafa M.; Ng, Seik Weng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 6
• Pages of publication: m791
• a: 8.7579 ± 0.0002 Å
• b: 10.6985 ± 0.0003 Å
• c: 15.3603 ± 0.0006 Å
• α: 72.079 ± 0.003°
• β: 77.582 ± 0.003°
• γ: 86.538 ± 0.002°
• Cell volume: 1337.31 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0287
• Residual factor for significantly intense reflections: 0.0239
• Weighted residual factors for significantly intense reflections: 0.0547
• Weighted residual factors for all reflections included in the refinement: 0.0572
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes