Information card for entry 2236306

Structure parameters

• Chemical name: 6,6'-Dimethoxy-2,2'-{[(<i>E</i>,<i>E</i>)-hydrazine-1,2- diylidene]bis(methanylylidene)}diphenol methanol disolvate
• Formula: C18 H24 N2 O6
• Calculated formula: C18 H24 N2 O6
• Title of publication: 6,6'-Dimethoxy-2,2'-{[(<i>E</i>,<i>E</i>)-hydrazine-1,2-diylidene]bis(methanylylidene)}diphenol methanol disolvate
• Authors of publication: Randell, Nicholas M.; Thompson, Laurence K.; Dawe, Louise N.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 9
• Pages of publication: o2711
• a: 20.517 ± 0.002 Å
• b: 4.8374 ± 0.0005 Å
• c: 21.366 ± 0.003 Å
• α: 90°
• β: 153.566 ± 0.007°
• γ: 90°
• Cell volume: 944 ± 0.3 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0698
• Residual factor for significantly intense reflections: 0.0619
• Weighted residual factors for significantly intense reflections: 0.1865
• Weighted residual factors for all reflections included in the refinement: 0.1944
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes