Information card for entry 2236346

Structure parameters

• Chemical name: Tris(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')cobalt(III) bis[bis(pyridine-2,6-dicarboxylato- κ^3^<i>O</i>^2^,<i>N</i>,<i>O</i>^6^)cobaltate(III)] perchlorate dimethylformamide hemisolvate 1.3-hydrate
• Formula: C59.5 H42.1 Cl Co3 N10.5 O21.8
• Calculated formula: C59.5 H42.1 Cl Co3 N10.5 O21.8
• Title of publication: Tris(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')cobalt(III) bis[bis(pyridine-2,6-dicarboxylato-κ^3^<i>O</i>^2^,<i>N</i>,<i>O</i>^6^)cobaltate(III)] perchlorate dimethylformamide hemisolvate 1.3-hydrate
• Authors of publication: Golenya, Irina A.; Boyko, Alexander N.; Kotova, Natalia V.; Haukka, Matti; Iskenderov, Turganbay S.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 10
• Pages of publication: m1237 - m1238
• a: 14.1988 ± 0.0004 Å
• b: 14.7317 ± 0.0006 Å
• c: 16.6016 ± 0.0008 Å
• α: 113.286 ± 0.002°
• β: 107.128 ± 0.003°
• γ: 90.19 ± 0.003°
• Cell volume: 3019.8 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0927
• Residual factor for significantly intense reflections: 0.0596
• Weighted residual factors for significantly intense reflections: 0.1605
• Weighted residual factors for all reflections included in the refinement: 0.181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes