Information card for entry 2236679

Structure parameters

• Chemical name: 2,2'-[(1<i>E</i>,2<i>E</i>)-1,2-Bis(hydroxyimino)ethane-1,2-diyl]dipyridinium hexachloridorhenate(IV)
• Formula: C12 H12 Cl6 N4 O2 Re
• Calculated formula: C12 H12 Cl6 N4 O2 Re
• Title of publication: 2,2'-[(1<i>E</i>,2<i>E</i>)-1,2-Bis(hydroxyimino)ethane-1,2-diyl]dipyridinium hexachloridorhenate(IV)
• Authors of publication: Krawczyk, Monika K.; Krawczyk, Marta S.; Siczek, Miłosz; Lis, Tadeusz
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 9
• Pages of publication: m1174 - m1175
• a: 7.836 ± 0.003 Å
• b: 8.051 ± 0.003 Å
• c: 8.733 ± 0.003 Å
• α: 85.44 ± 0.03°
• β: 73.85 ± 0.03°
• γ: 65.12 ± 0.04°
• Cell volume: 479.6 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0288
• Residual factor for significantly intense reflections: 0.0254
• Weighted residual factors for significantly intense reflections: 0.0379
• Weighted residual factors for all reflections included in the refinement: 0.0385
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes