Information card for entry 2237045

Structure parameters

• Chemical name: <i>trans</i>-Di-μ-chlorido-bis{chlorido[tris(3,5-dimethylphenyl)phosphane- κ<i>P</i>]palladium(II)} dichloromethane monosolvate
• Formula: C49 H56 Cl6 P2 Pd2
• Calculated formula: C49 H56 Cl6 P2 Pd2
• Title of publication: <i>trans</i>-Di-μ-chlorido-bis{chlorido[tris(3,5-dimethylphenyl)phosphane-κ<i>P</i>]palladium(II)} dichloromethane monosolvate
• Authors of publication: Davis, Wade L.; Muller, Alfred
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 12
• Pages of publication: m1563 - m1564
• a: 14.747 ± 0.002 Å
• b: 9.1038 ± 0.0013 Å
• c: 21.376 ± 0.003 Å
• α: 90°
• β: 117.576 ± 0.008°
• γ: 90°
• Cell volume: 2543.8 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.0981
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes