Information card for entry 2237087

Structure parameters

• Chemical name: μ-Carbonato-κ^4^<i>O</i>,<i>O</i>':<i>O</i>',<i>O</i>''-bis{[2'-(di- <i>tert</i>-butylphosphanyl)biphenyl-2-yl- κ^2^<i>P</i>,<i>C</i>^1^]palladium(II)} dichloromethane monosolvate
• Formula: C42 H54 Cl2 O3 P2 Pd2
• Calculated formula: C42 H54 Cl2 O3 P2 Pd2
• Title of publication: μ-Carbonato-κ^4^<i>O</i>,<i>O</i>':<i>O</i>',<i>O</i>''-bis{[2'-(di-<i>tert</i>-butylphosphanyl)biphenyl-2-yl-κ^2^<i>P</i>,<i>C</i>^1^]palladium(II)} dichloromethane monosolvate
• Authors of publication: Muller, Alfred; Holzapfel, Cedric W.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 12
• Pages of publication: m1574 - m1575
• a: 7.5459 ± 0.0006 Å
• b: 14.6579 ± 0.0011 Å
• c: 18.7078 ± 0.0014 Å
• α: 83.866 ± 0.002°
• β: 86.457 ± 0.002°
• γ: 86.478 ± 0.002°
• Cell volume: 2050.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0257
• Residual factor for significantly intense reflections: 0.0195
• Weighted residual factors for all reflections included in the refinement: 0.0441
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes