Information card for entry 2237096

Structure parameters

• Chemical name: <i>trans</i>-Dichloridobis{tris[4-(trifluoromethyl)phenyl]phosphane- κ<i>P</i>}palladium(II) dichloromethane monosolvate
• Formula: C43 H26 Cl4 F18 P2 Pd
• Calculated formula: C43 H26 Cl4 F18 P2 Pd
• Title of publication: <i>trans</i>-Dichloridobis{tris[4-(trifluoromethyl)phenyl]phosphane-κ<i>P</i>}palladium(II) dichloromethane monosolvate
• Authors of publication: Davis, Wade L.; Muller, Alfred
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2012
• Journal volume: 68
• Journal issue: 12
• Pages of publication: m1508 - m1509
• a: 12.1491 ± 0.001 Å
• b: 14.0203 ± 0.0013 Å
• c: 14.4334 ± 0.0013 Å
• α: 72.764 ± 0.002°
• β: 78.362 ± 0.002°
• γ: 75.545 ± 0.002°
• Cell volume: 2252 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0718
• Weighted residual factors for all reflections included in the refinement: 0.0767
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes