Information card for entry 2237119

Structure parameters

• Chemical name: <i>catena</i>-Poly[[[<i>O</i>,<i>O</i>'-bis(2-methylphenyl) dithiophosphato- κ^2^<i>S</i>,<i>S</i>]lead(II)]-μ-<i>O</i>,<i>O</i>'-bis(2-methylphenyl) dithiophosphato-κ^3^<i>S</i>,<i>S</i>':<i>S</i>]
• Formula: C28 H28 O4 P2 Pb S4
• Calculated formula: C28 H28 O4 P2 Pb S4
• Title of publication: <i>catena</i>-Poly[[[<i>O</i>,<i>O</i>'-bis(2-methylphenyl) dithiophosphato-κ^2^<i>S</i>,<i>S</i>]lead(II)]-μ-<i>O</i>,<i>O</i>'-bis(2-methylphenyl) dithiophosphato-κ^3^<i>S</i>,<i>S</i>':<i>S</i>]
• Authors of publication: Butcher, Ray J.; Ratnani, Raju; Öztürk Yildirim, Sema; Falola, Oluwaseun
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 1
• Pages of publication: m29 - m30
• a: 12.0263 ± 0.0006 Å
• b: 10.742 ± 0.0004 Å
• c: 13.0499 ± 0.0008 Å
• α: 90°
• β: 112.849 ± 0.006°
• γ: 90°
• Cell volume: 1553.58 ± 0.15 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0326
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.0731
• Weighted residual factors for all reflections included in the refinement: 0.075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes