Information card for entry 2237227

Structure parameters

• Chemical name: μ-Azido-κ^2^<i>N</i>^1^:<i>N</i>^1^-μ-chlorido-bis[(2-chloro-3- dimethylamino-1-phenylprop-1-en-1-yl-κ^2^<i>C</i>^1^,<i>N</i>)palladium(II)] chloroform monosolvate
• Formula: C23 H27 Cl6 N5 Pd2
• Calculated formula: C23 H27 Cl6 N5 Pd2
• SMILES: [Pd]12(C(c3ccccc3)=C(Cl)C[N]2(C)C)[Cl][Pd]2([N]1=N#N)[N](CC(=C2c1ccccc1)Cl)(C)C.ClC(Cl)Cl
• Title of publication: μ-Azido-κ^2^<i>N</i>^1^:<i>N</i>^1^-μ-chlorido-bis[(2-chloro-3-dimethylamino-1-phenylprop-1-en-1-yl-κ^2^<i>C</i>^1^,<i>N</i>)palladium(II)] chloroform monosolvate
• Authors of publication: Mafud, Ana C.; Oliviera, Milene A. R.; Gambardella, Maria T. P.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 1
• Pages of publication: m15
• a: 15.416 ± 0.003 Å
• b: 11.474 ± 0.003 Å
• c: 17.094 ± 0.004 Å
• α: 90°
• β: 97.14 ± 0.02°
• γ: 90°
• Cell volume: 3000.2 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2376
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for all reflections included in the refinement: 0.1697
• Goodness-of-fit parameter for all reflections included in the refinement: 0.932
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes