Information card for entry 2237318

Structure parameters

• Chemical name: (Acetonitrile){2-[bis(pyridin-2-ylmethyl-κ^2^<i>N</i>)amino-κ<i>N</i>]- <i>N</i>-(2,6-dimethylphenyl)acetamide-κ<i>O</i>}(perchlorato-κ<i>O</i>)zinc (acetonitrile){2-[bis(pyridin-2-ylmethyl-κ^2^<i>N</i>)amino-κ<i>N</i>]- <i>N</i>-(2,6-dimethylphenyl)acetamide-κ<i>O</i>}zinc tris(perchlorate)
• Formula: C48 H54 Cl4 N10 O18 Zn2
• Calculated formula: C48 H54 Cl4 N10 O18 Zn2
• Title of publication: (Acetonitrile){2-[bis(pyridin-2-ylmethyl-κ^2^<i>N</i>)amino-κ<i>N</i>]-<i>N</i>-(2,6-dimethylphenyl)acetamide-κ<i>O</i>}(perchlorato-κ<i>O</i>)zinc (acetonitrile){2-[bis(pyridin-2-ylmethyl-κ^2^<i>N</i>)amino-κ<i>N</i>]-<i>N</i>-(2,6-dimethylphenyl)acetamide-κ<i>O</i>}zinc tris(perchlorate)
• Authors of publication: Åstrand, Ove Alexander Høgmoen; Görbitz, Carl Henrik; Kristoffersen, Kenneth Aase; Rongved, Pål
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 2
• Pages of publication: m112 - m113
• a: 41.253 ± 0.008 Å
• b: 15.057 ± 0.003 Å
• c: 20.809 ± 0.004 Å
• α: 90°
• β: 106.106 ± 0.002°
• γ: 90°
• Cell volume: 12418 ± 4 ų
• Cell temperature: 105 ± 2 K
• Ambient diffraction temperature: 105 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1166
• Weighted residual factors for all reflections included in the refinement: 0.1241
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes