Information card for entry 2237906

Structure parameters

• Chemical name: <i>cyclo</i>-Tetrakis(μ~2~-<i>D</i>-penicillaminato-κ^4^<i>N</i>,<i>S</i>:<i>O</i>,<i>S</i>)tetrapalladium(II) 9.75-hydrate
• Formula: C20 H55.5 N4 O17.75 Pd4 S4
• Calculated formula: C20 H55.5 N4 O17.75 Pd4 S4
• Title of publication: <i>cyclo</i>-Tetrakis(μ~2~-<small>D</small>-penicillaminato-κ^4^<i>N</i>,<i>S</i>:<i>O</i>,<i>S</i>)tetrapalladium(II) 9.75-hydrate
• Authors of publication: Yokoi, Anzu; Yoshinari, Nobuto; Konno, Takumi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 5
• Pages of publication: m288 - m289
• a: 12.4517 ± 0.0003 Å
• b: 13.268 ± 0.0004 Å
• c: 15.1666 ± 0.0011 Å
• α: 113.527 ± 0.008°
• β: 98.425 ± 0.007°
• γ: 108.557 ± 0.008°
• Cell volume: 2067.3 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0259
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for significantly intense reflections: 0.0614
• Weighted residual factors for all reflections included in the refinement: 0.0621
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes