Information card for entry 2238496

Structure parameters

• Chemical name: Bis[<i>O</i>,<i>O</i>'-bis(4-<i>tert</i>-butylphenyl) dithiophosphato-κ^2^<i>S</i>,<i>S</i>']bis(pyridine-κ<i>N</i>)lead(II)
• Formula: C50 H62 N2 O4 P2 Pb S4
• Calculated formula: C50 H62 N2 O4 P2 Pb S4
• Title of publication: Bis[<i>O</i>,<i>O</i>'-bis(4-<i>tert</i>-butylphenyl) dithiophosphato-κ^2^<i>S</i>,<i>S</i>']bis(pyridine-κ<i>N</i>)lead(II)
• Authors of publication: Zhang, Xiulan; Xie, Bin; He, Linxin; Lu, Lu; Chen, Neng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 9
• Pages of publication: m524
• a: 12.426 ± 0.0003 Å
• b: 12.9136 ± 0.0003 Å
• c: 17.9749 ± 0.0004 Å
• α: 89.7528 ± 0.0018°
• β: 79.4467 ± 0.0019°
• γ: 71.298 ± 0.002°
• Cell volume: 2681.23 ± 0.11 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0462
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0619
• Weighted residual factors for all reflections included in the refinement: 0.0675
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes