Information card for entry 2239116

Structure parameters

• Chemical name: 1,1'-(Diselanediylbis{[<i>P</i>,<i>P</i>-diphenyl-<i>N</i>-(trimethylsilyl)phosphorimidoyl]methanylylidene})bis[1,1-diphenyl-<i>N</i>-(trimethylsilyl)-λ^5^-phosphanamine] pentane disolvate
• Formula: C72 H102 N4 P4 Se2 Si4
• Calculated formula: C62 H78 N4 P4 Se2 Si4
• Title of publication: 1,1'-(Diselanediylbis{[<i>P</i>,<i>P</i>-diphenyl-<i>N</i>-(trimethylsilyl)phosphorimidoyl]methanylylidene})bis[1,1-diphenyl-<i>N</i>-(trimethylsilyl)-λ^5^-phosphanamine] pentane disolvate
• Authors of publication: Thirumoorthi, Ramalingam; Chivers, Tristram; Laitinen, Risto S.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 1
• Pages of publication: o20 - o21
• a: 10.25 ± 0.0003 Å
• b: 13.442 ± 0.0003 Å
• c: 14.667 ± 0.0004 Å
• α: 65.611 ± 0.001°
• β: 85.525 ± 0.001°
• γ: 76.73 ± 0.002°
• Cell volume: 1791.03 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0882
• Residual factor for significantly intense reflections: 0.0683
• Weighted residual factors for significantly intense reflections: 0.1573
• Weighted residual factors for all reflections included in the refinement: 0.1695
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes