Information card for entry 2239634

Structure parameters

• Chemical name: μ~2~-Acetato-κ^2^<i>O</i>:<i>O</i>'-(4,4'-bipyridyl-κ<i>N</i>)tris(diethyl dithiophosphato-κ^2^<i>S</i>,<i>S</i>')-μ~3~-sulfido-tri-μ~2~-sulfido-trimolybdenum(V) diethyl ether solvate
• Formula: C28 H51 Mo3 N2 O9 P3 S10
• Calculated formula: C28 H51 Mo3 N2 O9 P3 S10
• Title of publication: μ~2~-Acetato-κ^2^<i>O</i>:<i>O</i>'-(4,4'-bipyridyl-κ<i>N</i>)tris(diethyl dithiophosphato-κ^2^<i>S</i>,<i>S</i>')-μ~3~-sulfido-tri-μ~2~-sulfido-trimolybdenum(IV) diethyl ether monosolvate
• Authors of publication: Kawamoto, Keisuke; Kinoshita, Isamu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 7
• Pages of publication: m240 - m241
• a: 13.1573 ± 0.0016 Å
• b: 27.647 ± 0.003 Å
• c: 14.2153 ± 0.0017 Å
• α: 90°
• β: 107.718 ± 0.0016°
• γ: 90°
• Cell volume: 4925.7 ± 1 ų
• Cell temperature: 153 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for all reflections included in the refinement: 0.0945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes