Information card for entry 2239996

Structure parameters

• Chemical name: Poly[aquabis(μ-nitrato-κ^4^<i>O</i>,<i>O</i>':<i>O</i>,<i>O</i>'')tetrakis(nitrato-κ^2^<i>O</i>,<i>O</i>'){μ~4~-tetraethyl [(ethane-1,2-diyl)bis(azanediyl)bis(2-oxoethane-2,1-diyl)]diphosphonate-κ^2^<i>O</i>,<i>O</i>'}disamarium(III)]
• Formula: C14 H32 N8 O27 P2 Sm2
• Calculated formula: C14 H32 N8 O27 P2 Sm2
• Title of publication: Crystal structure of a samarium(III) nitrate chain cross-linked by a bis-carbamoylmethylphosphine oxide ligand
• Authors of publication: Stoscup, Julie A.; Staples, Richard J.; Biros, Shannon M.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 10
• Pages of publication: 188 - 191
• a: 8.9416 ± 0.0007 Å
• b: 11.0128 ± 0.0009 Å
• c: 18.4635 ± 0.0015 Å
• α: 81.441 ± 0.001°
• β: 83.428 ± 0.001°
• γ: 86.977 ± 0.001°
• Cell volume: 1784.9 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0324
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for significantly intense reflections: 0.0645
• Weighted residual factors for all reflections included in the refinement: 0.0679
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes