Information card for entry 2240028

Structure parameters

• Chemical name: <i>trans</i>-Difluoridotetrakis-(pyridine-κ<i>N</i>)chromium(III) trichlorido(pyridine-κ<i>N</i>)zincate monohydrate
• Formula: C25 H27 Cl3 Cr F2 N5 O Zn
• Calculated formula: C25 H27 Cl3 Cr F2 N5 O Zn
• Title of publication: Crystal structure of <i>trans</i>-difluoridotetrakis(pyridine-κ<i>N</i>)chromium(III) trichlorido(pyridine-κ<i>N</i>)zincate monohydrate from synchrotron data
• Authors of publication: Moon, Dohyun; Choi, Jong-Ha
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 11
• Pages of publication: 290 - 293
• a: 9.135 ± 0.0018 Å
• b: 12.852 ± 0.003 Å
• c: 13.607 ± 0.003 Å
• α: 103.69 ± 0.03°
• β: 105.07 ± 0.03°
• γ: 101.25 ± 0.03°
• Cell volume: 1441.6 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0379
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0991
• Weighted residual factors for all reflections included in the refinement: 0.0996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.62998 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes