Information card for entry 2240381

Structure parameters

• Chemical name: Bis(2,2'-bipyridine)[<i>N</i>'-(quinolin-2-ylmethylidene)pyridine-\ 2-carbohydrazide]ruthenium(II) bis(tetrafluoridoborate) dichloromethane trisolvate
• Formula: C39 H34 B2 Cl6 F8 N8 O Ru
• Calculated formula: C39 H34 B2 Cl6 F8 N8 O Ru
• SMILES: [Ru]123([O]=C(N[N]1=Cc1nc4ccccc4cc1)c1ncccc1)([n]1ccccc1c1[n]2cccc1)[n]1ccccc1c1[n]3cccc1.ClCCl.ClCCl.ClCCl.[B](F)(F)(F)[F-].[B](F)(F)(F)[F-]
• Title of publication: Crystal structure of bis(2,2'-bipyridine)[<i>N</i>'-(quinolin-2-ylmethylidene)pyridine-2-carbohydrazide]ruthenium(II) bis(tetrafluoridoborate) dichloromethane trisolvate
• Authors of publication: Mori, Asami; Suzuki, Takayoshi; Nakajima, Kiyohiko
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2015
• Journal volume: 71
• Journal issue: 2
• Pages of publication: 142 - 145
• a: 11.0165 ± 0.0012 Å
• b: 13.2508 ± 0.0015 Å
• c: 16.4285 ± 0.0019 Å
• α: 77.812 ± 0.004°
• β: 76.924 ± 0.004°
• γ: 88.367 ± 0.004°
• Cell volume: 2282.9 ± 0.4 ų
• Cell temperature: 192 ± 2 K
• Ambient diffraction temperature: 192 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.0686
• Weighted residual factors for significantly intense reflections: 0.1955
• Weighted residual factors for all reflections included in the refinement: 0.2076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes