Information card for entry 2241008

Structure parameters

• Chemical name: Sodium potassium hexa-μ~3~-hydroxido-μ~2~-hydroxido-heptadecaoxidocobaltate(II)hexamolybdate(VI) octahydrate
• Formula: Co H23 K Mo6 Na O32
• Calculated formula: Co H23 K Mo6 Na O32
• Title of publication: Crystal structure of potassium sodium heptahydrogen hexamolybdocobaltate(III) octahydrate: an extra-protonated <i>B</i>-series Anderson-type heteropolyoxidometalate
• Authors of publication: Park, Ki-Min; Joo, Hea-Chung; Lee, Uk
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2015
• Journal volume: 71
• Journal issue: 9
• Pages of publication: 1032 - 1035
• a: 10.9758 ± 0.0005 Å
• b: 20.7702 ± 0.0009 Å
• c: 12.7906 ± 0.0006 Å
• α: 90°
• β: 99.666 ± 0.001°
• γ: 90°
• Cell volume: 2874.5 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0775
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.0713
• Weighted residual factors for all reflections included in the refinement: 0.0808
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes