Information card for entry 2241372

Structure parameters

• Common name: sjfbk16
• Chemical name: Tris[1-oxopyridine-2-olato(1-)]silicon(IV) chloride chloroform-<i>d</i>~1~ disolvate
• Formula: C17 H12 Cl7 D2 N3 O6 Si
• Calculated formula: C17 H12 Cl7 D2 N3 O6 Si
• Title of publication: Crystal structures of tris[1-oxopyridine-2-olato(1{-})]silicon(IV) chloride chloroform-<i>d</i>~1~ disolvate, tris[1-oxopyridine-2-olato(1{-})]silicon(IV) chloride acetonitrile unquantified solvate, and <i>fac</i>-tris[1-oxopyridine-2-thiolato(1{-})]silicon(IV) chloride chloroform-<i>d</i>~1~ disolvate
• Authors of publication: Kraft, Bradley M.; Brennessel, William W.; Ryan, Amy E.; Benjamin, Candace K.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2015
• Journal volume: 71
• Journal issue: 12
• Pages of publication: 1531 - 1535
• a: 13.5133 ± 0.0007 Å
• b: 13.5039 ± 0.0007 Å
• c: 13.7752 ± 0.0007 Å
• α: 90°
• β: 101.866 ± 0.001°
• γ: 90°
• Cell volume: 2460 ± 0.2 ų
• Cell temperature: 100 ± 0.5 K
• Ambient diffraction temperature: 100 ± 0.5 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1025
• Weighted residual factors for all reflections included in the refinement: 0.117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes