Crystal structure of {6,6'-dibenzoyl-4,4'-di-<i>tert</i>-butyl-2,2'-[(ethane-1,2-diyl)dinitrilobis(phenylmethanylylidene)]diphenolato-κ^4^<i>O</i>^1^,<i>N</i>,<i>N</i>',<i>O</i>^1'^}nickel(II)
Authors of publication
Gupta, Abhishek K.; Butcher, Ray J.; Sil, Anjan
Journal of publication
Acta Crystallographica Section E
Year of publication
2015
Journal volume
71
Journal issue
12
Pages of publication
1485 - 1487
a
12.4401 ± 0.0009 Å
b
16.8987 ± 0.0011 Å
c
21.5185 ± 0.0012 Å
α
100.843 ± 0.005°
β
100.029 ± 0.006°
γ
99.89 ± 0.006°
Cell volume
4276.1 ± 0.5 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1228
Residual factor for significantly intense reflections
0.0676
Weighted residual factors for significantly intense reflections
0.1578
Weighted residual factors for all reflections included in the refinement
0.2076
Goodness-of-fit parameter for all reflections included in the refinement
