Information card for entry 2241926

Structure parameters

• Chemical name: Di-μ-iodido-bis[({4-amino-1,5-bis[2,6-bis(propan-2-yl)phenyl]pent-3-en-2-ylidene}azanido-κ^2^<i>N</i>,<i>N</i>')magnesium(II] toluene sesquisolvate
• Formula: C68.5 H94 I2 Mg2 N4
• Calculated formula: C68.5 H94 I2 Mg2 N4
• Title of publication: Crystal structure of a dimeric β-diketiminate magnesium complex
• Authors of publication: MacNeil, Connor S.; Johnson, Kevin R. D.; Hayes, Paul G.; Boeré, René T.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 12
• Pages of publication: 1754 - 1756
• a: 19.1596 ± 0.0015 Å
• b: 21.0532 ± 0.0016 Å
• c: 16.5711 ± 0.0013 Å
• α: 90°
• β: 99.935 ± 0.0008°
• γ: 90°
• Cell volume: 6584.1 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0339
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0837
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes