Information card for entry 2241943

Structure parameters

• Chemical name: Tetrakis[μ~3~-4-methyl-<i>N</i>-(2-oxidophenyl)salicylideneiminato]tetrakis[methanolnickel(II)] methanol 0.8-solvate
• Formula: C60.8 H63.2 N4 Ni4 O12.8
• Calculated formula: C60.8 H63.2 N4 Ni4 O12.8
• Title of publication: A tetranuclear cubane-like nickel(II) complex with a tridentate salicylideneimine Schiff base ligand: tetrakis[μ~3~-4-methyl-<i>N</i>-(2-oxidophenyl)salicylideneiminato]tetrakis[methanolnickel(II)] methanol 0.8-solvate
• Authors of publication: Pavlović, Gordana; Majer, Mihael; Cindrić, Marina
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 12
• Pages of publication: 1776 - 1779
• a: 22.581 ± 0.0005 Å
• b: 13.7701 ± 0.0003 Å
• c: 18.5242 ± 0.0004 Å
• α: 90°
• β: 92.125 ± 0.002°
• γ: 90°
• Cell volume: 5756 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1432
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1301
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes