Information card for entry 2242192

Structure parameters

• Chemical name: <i>cis</i>-(<i>N</i>-{2-[2,6-bis(propan-2-yl)phenylimino]pentan-3-ylidene}-\ 2,6-bis(propan-2-yl)aniline)dichloridopalladium(II) 1,2-dichloroethane monosolvate
• Formula: C31 H46 Cl4 N2 Pd
• Calculated formula: C31 H46 Cl4 N2 Pd
• Title of publication: Crystal structure of unsymmetrical α-diimine palladium(II) complex <i>cis</i>-[{ArN=C(Me)‒(Et)C=NAr}PdCl~2~] [Ar = 2,6-(iPr)~2~C~6~H~3~]
• Authors of publication: Ellandula, Shravan Kumar; Opoku Amoako, Cosmos; Mague, Joel T.; Chandrasekaran, Perumalreddy
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2017
• Journal volume: 73
• Journal issue: 8
• Pages of publication: 1148 - 1150
• a: 8.7203 ± 0.0012 Å
• b: 20.124 ± 0.003 Å
• c: 19.526 ± 0.003 Å
• α: 90°
• β: 100.405 ± 0.002°
• γ: 90°
• Cell volume: 3370.2 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0763
• Weighted residual factors for all reflections included in the refinement: 0.0841
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes