Information card for entry 2243058

Structure parameters

• Chemical name: {[2-(Anthracen-9-yl)phenolato-κ<i>O</i>]bis(tetrahydrofuran)ytterbium(III)}-tris[μ-2-(anthracen-9-yl)phenolato]-κ^2^<i>O</i>:<i>O</i>;κ^2^<i>O</i>:<i>O</i>;κ<i>O</i>:1,2-η,κ<i>O</i>]-{[2-(anthracen-9-yl)phenolato-κ<i>O</i>]ytterbium(II)} toluene trisolvate
• Formula: C129 H105 O7 Yb2
• Calculated formula: C129 H105 O7 Yb2
• Title of publication: Crystal structure of a binuclear mixed-valence ytterbium complex containing a 2-anthracene-substituted phenoxide ligand
• Authors of publication: Berg, David J.; Twamley, Brendan
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2019
• Journal volume: 75
• Journal issue: 9
• Pages of publication: 1367 - 1371
• a: 14.4612 ± 0.0007 Å
• b: 20.8473 ± 0.001 Å
• c: 32.0864 ± 0.0015 Å
• α: 90°
• β: 95.508 ± 0.001°
• γ: 90°
• Cell volume: 9628.6 ± 0.8 ų
• Cell temperature: 83 ± 2 K
• Ambient diffraction temperature: 83 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0756
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes