Crystal structures of [(μ~2~-L1)dibromidodicopper(II)] dibromide and poly[[(μ~2~-L1)diiodidodicopper(I)]-di-μ-iodido-dicopper(I)], where L1 is 2,5,8,11,14,17-hexathia-[9.9](2,6,3,5)-pyrazinophane
Authors of publication
Assoumatine, Tokouré; Stoeckli-Evans, Helen
Journal of publication
Acta Crystallographica Section E
Year of publication
2020
Journal volume
76
Journal issue
7
Pages of publication
984 - 989
a
7.7713 ± 0.0008 Å
b
8.9456 ± 0.0009 Å
c
11.2464 ± 0.0014 Å
α
106.839 ± 0.013°
β
104.644 ± 0.013°
γ
93.412 ± 0.012°
Cell volume
716.53 ± 0.16 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0923
Residual factor for significantly intense reflections
0.0699
Weighted residual factors for significantly intense reflections
0.176
Weighted residual factors for all reflections included in the refinement
0.1834
Goodness-of-fit parameter for all reflections included in the refinement