Information card for entry 2243977

Structure parameters

• Chemical name: Bis[3,5-bis(trifluoromethyl)phenyl-2κ<i>C</i>^1^](fluorido-1κ<i>I</i>)(hydrido-2κ<i>H</i>)bis[1,1(η^5^)-pentamethylcyclopentadienyl]germaniumuranium(<i>Ge</i>—<i>U</i>)
• Formula: C37 H39 F13 Ge U
• Calculated formula: C37 H39 F13 Ge U
• Title of publication: Crystal structures of metallocene complexes with uranium–germanium bonds
• Authors of publication: Tarlton, Michael L.; Kelley, Steven P.; Walensky, Justin R.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2021
• Journal volume: 77
• Journal issue: 12
• Pages of publication: 1258 - 1262
• a: 34.16 ± 0.003 Å
• b: 13.5237 ± 0.0011 Å
• c: 16.2986 ± 0.0013 Å
• α: 90°
• β: 95.028 ± 0.002°
• γ: 90°
• Cell volume: 7500.5 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0736
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0838
• Weighted residual factors for all reflections included in the refinement: 0.0941
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes