Synthesis, crystal structure and Hirshfeld surface analysis of dimethyl 3-(3-bromophenyl)-6-methyl-7-oxo-3,5,6,7-tetrahydropyrazolo[1,2-<i>a</i>]pyrazole-1,2-dicarboxylate
Authors of publication
El Ajlaoui, Rahhal; Hakmaoui, Yassine; Rakib, El Mostapha; Ketatni, El Mostafa; Saadi, Mohamed; El Ammari, Lahcen
Journal of publication
Acta Crystallographica Section E
Year of publication
2022
Journal volume
78
Journal issue
2
a
8.8579 ± 0.0005 Å
b
10.5336 ± 0.0006 Å
c
11.0893 ± 0.0006 Å
α
62.282 ± 0.002°
β
75.437 ± 0.002°
γ
88.241 ± 0.002°
Cell volume
882.03 ± 0.09 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0355
Residual factor for significantly intense reflections
0.0274
Weighted residual factors for significantly intense reflections
0.0738
Weighted residual factors for all reflections included in the refinement
0.0781
Goodness-of-fit parameter for all reflections included in the refinement
