Information card for entry 2311341

Structure parameters

• Chemical name: Tris(3-phenyl-<i>N</i>,<i>N</i>'-dicyclohexylpropynamidinato-κ^2^<i>N</i>,<i>N</i>')ytterbium(III)
• Formula: C63 H81 N6 Yb
• Calculated formula: C63 H81 N6 Yb
• Title of publication: Crystal structures of two ytterbium(III) complexes comprising alkynylamidinate ligands.
• Authors of publication: Wang, Sida; Sroor, Farid M.; Liebing, Phil; Lorenz, Volker; Hilfert, Liane; Edelmann, Frank T.
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2016
• Journal volume: 72
• Journal issue: Pt 9
• Pages of publication: 1229 - 1233
• a: 20.3469 ± 0.0003 Å
• b: 20.3469 ± 0.0003 Å
• c: 50.3074 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 18036.8 ± 0.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.0404
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0663
• Weighted residual factors for all reflections included in the refinement: 0.0712
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No