Information card for entry 2311350

Structure parameters

• Chemical name: Poly[bis(μ~3~-cyanido-κ^3^<i>C</i>:<i>C</i>:<i>N</i>)tris(μ~2~-cyanido-κ^2^<i>C</i>:<i>N</i>)bis(<i>N</i>-methylethane-1,2-diamine\- κ^2^<i>N</i>,<i>N</i>')tricopper(I)copper(II)]
• Formula: C11 H20 Cu4 N9
• Calculated formula: C11 H20 Cu4 N9
• Title of publication: Crystal structures of two mixed-valence copper cyanide complexes with <i>N</i>-methyl-ethylenedi-amine.
• Authors of publication: Corfield, Peter W. R.; Sabatino, Alexander
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2017
• Journal volume: 73
• Journal issue: Pt 2
• Pages of publication: 141 - 146
• a: 19.509 ± 0.002 Å
• b: 8.2306 ± 0.0013 Å
• c: 11.1 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1782.3 ± 0.5 ų
• Cell temperature: 303 ± 2 K
• Ambient diffraction temperature: 303 ± 1 K
• Number of distinct elements: 4
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0189
• Residual factor for significantly intense reflections: 0.018
• Weighted residual factors for significantly intense reflections: 0.0445
• Weighted residual factors for all reflections included in the refinement: 0.0447
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No