Information card for entry 2311449

Structure parameters

• Chemical name: μ~2~-Chlorido-dichlorido(μ~2~-2-{[2-(dimethylamino)ethyl]iminomethyl}phenolato)(<i>N</i>,<i>N</i>-dimethylethylenediamine)dicopper(II) 0.11-hydrate
• Formula: C15 H27.22 Cl3 Cu2 N4 O1.11
• Calculated formula: C15 H27 Cl3 Cu2 N4 O1.108
• Title of publication: <i>N</i>,<i>N</i>',<i>N</i>'' <i>versus N</i>,<i>N</i>',<i>O</i> imine-containing coordination motifs: ligand-directed synthesis of mononuclear and binuclear Cu^II compounds.
• Authors of publication: Ferraz de Paiva, Raphael Enoque; Nakahata, Douglas Hideki; de Carvalho, Marcos Alberto; Rodrigues Goulart Bergamini, Fernando; Corbi, Pedro Paulo
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2017
• Journal volume: 73
• Journal issue: Pt 10
• Pages of publication: 1563 - 1567
• a: 11.0838 ± 0.0004 Å
• b: 18.0949 ± 0.0007 Å
• c: 10.661 ± 0.0004 Å
• α: 90°
• β: 101.474 ± 0.002°
• γ: 90°
• Cell volume: 2095.44 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0256
• Residual factor for significantly intense reflections: 0.022
• Weighted residual factors for significantly intense reflections: 0.0545
• Weighted residual factors for all reflections included in the refinement: 0.0562
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No