Information card for entry 2311480

Structure parameters

• Chemical name: Aqua(perchlorato)bis[μ-(<i>E</i>)-2-({[2-(pyridin-2-yl)ethyl]imino}methyl)phenolato-κ^4^<i>N</i>,<i>N</i>',<i>O</i>:<i>O</i>]dicopper(II) perchlorate
• Formula: C28 H28 Cl2 Cu2 N4 O11
• Calculated formula: C28 H28 Cl2 Cu2 N4 O11
• Title of publication: Crystal structure of aqua-(perchlorato)bis-[μ-(<i>E</i>)-2-({[2-(pyridin-2-yl)eth-yl]imino}-meth-yl)phenolato-κ⁴<i>N</i>,<i>N</i>',<i>O</i>:<i>O</i>]dicopper(II) perchlorate.
• Authors of publication: Okeke, Ugochukwu; Gultneh, Yilma; Butcher, Ray J.
• Journal of publication: Acta crystallographica. Section E, Crystallographic communications
• Year of publication: 2017
• Journal volume: 73
• Journal issue: Pt 11
• Pages of publication: 1708 - 1711
• a: 7.4829 ± 0.0004 Å
• b: 16.8867 ± 0.0008 Å
• c: 24.2649 ± 0.0013 Å
• α: 90°
• β: 98.18 ± 0.003°
• γ: 90°
• Cell volume: 3035 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0773
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No