Crystallography Open Database

Information card for entry 2311870

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Coordinates	2311870.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Vinylpyridine lithium chloride solvate
Chemical name	Di-μ-chlorido-bis[bis(4-ethenylpyridine-κ<i>N</i>)lithium]
Formula	C28 H28 Cl2 Li2 N4
Calculated formula	C28 H28 Cl2 Li2 N4
Title of publication	Structure of salts of lithium chloride and lithium hexafluorophosphate as solvates with pyridine and vinylpyridine and structural comparisons: (C<sub>5</sub>H<sub>5</sub>N)LiPF<sub>6</sub>, [p-(CH<sub>2</sub>=CH)C<sub>5</sub>H<sub>4</sub>N]LiPF<sub>6</sub>, [(C<sub>5</sub>H<sub>5</sub>N)LiCl]<sub>n</sub>, and [p-(CH<sub>2</sub>=CH)C<sub>5</sub>H<sub>4</sub>N]<sub>2</sub>Li(μ-Cl)<sub>2</sub>Li[p-(CH<sub>2</sub>=CH)C<sub>5</sub>H<sub>4</sub>N]<sub>2</sub>.
Authors of publication	Jalil, AbdelAziz; Clymer, Rebecca N.; Hamilton, Clifton R.; Vaddypally, Shivaiah; Gau, Michael R.; Zdilla, Michael J.
Journal of publication	Acta crystallographica. Section C, Structural chemistry
Year of publication	2017
Journal volume	73
Journal issue	Pt 3
Pages of publication	264 - 269
a	12.24 ± 0.004 Å
b	18.88 ± 0.006 Å
c	12.675 ± 0.004 Å
α	90°
β	105.864 ± 0.006°
γ	90°
Cell volume	2817.5 ± 1.6 Å³
Cell temperature	178 ± 2 K
Ambient diffraction temperature	178 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1288
Residual factor for significantly intense reflections	0.0525
Weighted residual factors for significantly intense reflections	0.0937
Weighted residual factors for all reflections included in the refinement	0.117
Goodness-of-fit parameter for all reflections included in the refinement	0.97
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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