Information card for entry 2311957

Structure parameters

• Chemical name: Poly[[μ~3~-iodido-tri-μ~2~-iodido-iodido[bis(1,10-phenanthroline)copper(I)]copper(I)copper(II)lead(II)] hemiiodine]
• Formula: C24 H16 Cu2 I6 N4 Pb
• Calculated formula: C24 H16 Cu2.0002 I6 N4 Pb
• Title of publication: Syntheses and crystal structures of two heterometallic iodoplumbates containing mixed-valence copper(I/II).
• Authors of publication: Fan, Le Qing; Zhu, Xiao Tong
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2017
• Journal volume: 73
• Journal issue: Pt 12
• Pages of publication: 1098 - 1103
• a: 17.5853 ± 0.0009 Å
• b: 18.1041 ± 0.0008 Å
• c: 13.0705 ± 0.0006 Å
• α: 90°
• β: 128.789 ± 0.005°
• γ: 90°
• Cell volume: 3243.5 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.063
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0759
• Weighted residual factors for all reflections included in the refinement: 0.0856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No