Syntheses and crystal structures of four 4-(4-nitro-phen-yl)piperazinium salts with hydrogen succinate, 4-amino-benzoate, 2-(4-chloro-phen-yl)acetate and 2,3,4,5,6-penta-fluoro-benzoate anions.
Authors of publication
Vinaya, ?; Basavaraju, Yeriyur B.; Yathirajan, Hemmige S.; Parkin, Sean
Journal of publication
Acta crystallographica. Section E, Crystallographic communications
Year of publication
2023
Journal volume
79
Journal issue
Pt 3
Pages of publication
151 - 156
a
25.2747 ± 0.0012 Å
b
8.0434 ± 0.0004 Å
c
15.6617 ± 0.0005 Å
α
90°
β
105.384 ± 0.002°
γ
90°
Cell volume
3069.9 ± 0.2 Å3
Cell temperature
90 ± 0.2 K
Ambient diffraction temperature
90 ± 0.2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.039
Residual factor for significantly intense reflections
0.0339
Weighted residual factors for significantly intense reflections
0.0848
Weighted residual factors for all reflections included in the refinement
0.089
Goodness-of-fit parameter for all reflections included in the refinement
