Proton tautomerism in 5-dimethylaminomethylidene-4-(o-,m-,p-hydroxyphenyl)amino-1,3-thiazol-2(5H)-ones: synthesis, crystal structure and spectroscopic studies.
Authors of publication
Pyrih, Andrii; Łapiński, Andrzej; Zięba, Sylwia; Mizera, Adam; Lesyk, Roman; Jaskolski, Mariusz; Gzella, Andrzej K.
Journal of publication
Acta crystallographica Section B, Structural science, crystal engineering and materials
Year of publication
2023
Journal volume
79
Journal issue
3
Pages of publication
220 - 232
a
20.7594 ± 0.0003 Å
b
11.8833 ± 0.0002 Å
c
13.3407 ± 0.0002 Å
α
90°
β
104.534 ± 0.002°
γ
90°
Cell volume
3185.7 ± 0.09 Å3
Cell temperature
130 ± 0.1 K
Ambient diffraction temperature
130 ± 0.1 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0497
Residual factor for significantly intense reflections
0.0415
Weighted residual factors for significantly intense reflections
0.1213
Weighted residual factors for all reflections included in the refinement
0.1271
Goodness-of-fit parameter for all reflections included in the refinement
