Information card for entry 2312125

Structure parameters

• Chemical name: Bis[tris(ethane-1,2-diamine-κ^2^<i>N</i>,<i>N</i>')cobalt(III)] trichloride tetrahydrate
• Formula: C6 H32 Cl3 Co N6 O4
• Calculated formula: C6 H32 Cl3 Co N6 O4
• Title of publication: Double-salt formation in crystal structures containing [Co(en)₃]Cl₃.
• Authors of publication: Kollitz, Megan R.; Lappin, A. Graham; Oliver, Allen G.
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 5
• Pages of publication: 164 - 169
• a: 11.3193 ± 0.0009 Å
• b: 11.3193 ± 0.0009 Å
• c: 15.4254 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1711.6 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 165
• Hermann-Mauguin space group symbol: P -3 c 1
• Hall space group symbol: -P 3 2"c
• Residual factor for all reflections: 0.0371
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections included in the refinement: 0.1005
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes