Information card for entry 2312128

Structure parameters

• Chemical name: Ammonium bis[tris(ethane-1,2-diamine-κ^2^<i>N</i>,<i>N</i>')cobalt(III)] heptachloride hexahydrate
• Formula: C12 H64 Cl7 Co2 N13 O6
• Calculated formula: C12 H64 Cl7 Co2 N13 O6
• Title of publication: Double-salt formation in crystal structures containing [Co(en)₃]Cl₃.
• Authors of publication: Kollitz, Megan R.; Lappin, A. Graham; Oliver, Allen G.
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 5
• Pages of publication: 164 - 169
• a: 11.4131 ± 0.0014 Å
• b: 11.4131 ± 0.0014 Å
• c: 15.578 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1757.3 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 165
• Hermann-Mauguin space group symbol: P -3 c 1
• Hall space group symbol: -P 3 2"c
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0644
• Weighted residual factors for all reflections included in the refinement: 0.0685
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes