Information card for entry 2312316

Structure parameters

• Chemical name: Bis(μ-anthracene-κ^2^<i>C</i>^9^:<i>C</i>^10^)dicopper bis[bis(tetrahydrofuran-κ<i>O</i>)potassium]
• Formula: C44 H52 Cu2 K2 O4
• Calculated formula: C44 H52 Cu2 K2 O4
• Title of publication: Crystal structure and synthesis of the bis(anthracene)dicuprate dianion as the dipotassium salt, [K(tetrahydrofuran)₂]₂[{Cu(9,10-η²-anthracene)}₂], the first anionic arene complex of copper.
• Authors of publication: Young, Jr, Victor G; Brennessel, William W.; Ellis, John E.
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 11
• Pages of publication: 456 - 463
• a: 9.6864 ± 0.0019 Å
• b: 10.484 ± 0.002 Å
• c: 10.658 ± 0.002 Å
• α: 66.22 ± 0.03°
• β: 89.67 ± 0.03°
• γ: 82.73 ± 0.03°
• Cell volume: 981.3 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0356
• Residual factor for significantly intense reflections: 0.0287
• Weighted residual factors for significantly intense reflections: 0.0687
• Weighted residual factors for all reflections included in the refinement: 0.0726
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes