Information card for entry 2312334

Structure parameters

• Chemical name: Chlorido[tris(pyridin-2-yl)amine-κ^2^<i>N</i>,<i>N</i>'][tris(pyridin-2-yl)amine-κ^3^<i>N</i>,<i>N</i>',<i>N</i>'']ruthenium(II) hexafluoridoantimonate chloroform monosolvate
• Formula: C31 H25 Cl4 F6 N8 Ru Sb
• Calculated formula: C31 H25 Cl4 F6 N8 Ru Sb
• Title of publication: Studies of κ²- and κ³-tripyridylamine complexes of ruthenium and π-stacking by pyridyls.
• Authors of publication: Faller, Jack; Chase, Kevin J.; Parr, Jonathan; Mercado, Brandon
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2023
• Journal volume: 79
• Journal issue: Pt 12
• Pages of publication: 491 - 496
• a: 8.3209 ± 0.0003 Å
• b: 27.3213 ± 0.001 Å
• c: 15.7839 ± 0.0006 Å
• α: 90°
• β: 99.554 ± 0.004°
• γ: 90°
• Cell volume: 3538.5 ± 0.2 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93.15 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.0739
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes