Information card for entry 2312473

Structure parameters

• Chemical name: Bis{hydrotris[3-(furan-2-yl)pyrazol-1-yl]borato}dysprosium(III) tetraphenylborate dichloromethane monosolvate
• Formula: C67 H54 B3 Cl2 Dy N12 O6
• Calculated formula: C67 H54 B3 Cl2 Dy N12 O6
• Title of publication: Borotropic shifting of the [hydrotris(2'-furyl)pyrazol-1-yl]borate ligand in high-coordinate lanthanide complexes.
• Authors of publication: Thomas, Jarrod R.; Sulway, Scott A.
• Journal of publication: Acta crystallographica. Section C, Structural chemistry
• Year of publication: 2024
• Journal volume: 80
• Journal issue: 5
• a: 12.1461 ± 0.0007 Å
• b: 16.1883 ± 0.0008 Å
• c: 17.1795 ± 0.001 Å
• α: 102.659 ± 0.002°
• β: 103.322 ± 0.002°
• γ: 95.948 ± 0.002°
• Cell volume: 3164.6 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.0977
• Weighted residual factors for all reflections included in the refinement: 0.1049
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No